Undergraduate

Instrumental Analysis Laboratory I (3rd sem.)

Electrogravimetric and coulometric determinations, applications of ion selective electrodes, potentiometric titrations, polarographic analysis, stripping voltammetry, extraction, gas chromatographic analysis.
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Instrumental Analysis II (Separation Techniques) (4th sem.)

Spectrometric techniques. Introduction to optical methods of analysis. Molecular absorption spectrometry, ultraviolet and visible spectrometry and applications. Lambert- Beer’s law, photometric error. Spectrometric titrations. Molecular Luminescence Spectrometry (molecular fluorescence, phosphorescence, chemiluminescence). Atomic Absorption Spectrometry. Atomic Emission Spectrometry (Flame Atomic Emission Spectrometry, Inductively Coupled Plasma– Atomic Emission Spectrometry). Atomic and molecular mass spectrometry (MS, ICP-MS, LC-MS, GC- MS). Theory of chromatographic separations. Liquid Chromatography, instrumentation (chromatographic columns, detectors). Liquid Chromatographic techniques: HPLC, Ion Chromatography, Size Exclusion chromatography. Supercritical fluid chromatography and extraction. Kinetic and enzymatic analytical methods.
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Instrumental Analysis II Laboratory II

Spectrometric determination of manganese in steel. Flame emission spectrometric determination of alkali and alkaline earth elements. Determination of zinc in insulin preparations by atomic absorption spectrometry. Determination of quinine in tonic water by Fluorescence. Determination of analgesics in pharmaceutical formulations by high performance liquid chromatography (HPLC). Kinetic determination of lactate dehydrogenase (LDH) activity.
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Advanced Analytical Chemistry

Modern chromatographic techniques. Specific spectroscopic techniques (ICP, XRF, etc.). Hyphenated techniques. Non-destructive analysis (surface characterization, special microscopy). Thermal characterization methods. Automated analysis. Atomic and molecular mass spectrometry.
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Quality Assurance in Analytical Laboratories – Accreditation (8th sem.) (opt.)

Introduction in quality systems (ISO, EN). Quality assurance in testing and calibration laboratories. Laboratory Accreditation Regulations and Criteria (ISO 17025). Calibration and control of analytical instruments and devices. Development of Analytical Methods. Validation and verification of analytical methods. Uncertainty estimation. Traceability of measurements. Chemical Metrology. Sampling and Applications. Laboratory accreditation – procedural guidelines. Case Studies.
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Postgraduate:

Spectrometry: Atomic Absorption Spectrometry
Spectrometry: Atomic Emission Spectrometry (FAES, ICP-OES)
Spectrometry: Mass Spectrometry and Hyphenated techniques (ICP-MS)
Separation Techniques: Hyphenated techniques (LC-MS, LC-MS/MS)
Quality Systems and Accreditation (ISO/IEC 17025, Accreditation)
Quality Systems and Accreditation (Measurement Uncertainty)
Quality Control of Materials (Metals, Alloys, Ceramics, Migration, XRF, ICP-OES) (opt.)
Quality Control of Food (Chemical Hazards, Risk Assessment) (opt.)
Quality Control of the Environment (Sampling, Monitoring, Elemental and Speciation Analysis, Chemometrics) (opt.)